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Catalytic cracking of endothermic fuels in coated tube reactor

LI Jia, ZOU Jijun, ZHANG Xiangwen, GUO Wei, MI Zhentao

《化学科学与工程前沿（英文）》 2008年 第2卷 第2期   页码 181-185 doi: 10.1007/s11705-008-0032-1

摘要： Suspensoid of HZSM-5 or HY zeolites mixed with a self-made ceramic-like binder was coated on the inner wall of a tubular reactor by gas-aided fluid displacement technology. The coated zeolites were characterized by means of X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM). The coating thickness is 10–20 ?m and the particle size of the zeolites is in the range of 1–5 ?m. In the coated reactor, cracking of endothermic fuels including -dodecane and aviation fuel RP-3 was carried out separately under supercritical conditions at 600°C and 625°C to investigate their heat sinks and conversion of catalytic reactions. For the reaction catalyzed by HY(25% mass fraction) coating, the heat sink capacity of -dodecane are 815.7 and 901.9 kJ/kg higher than that of the bare tube at 600°C and at 625°C, respectively. Conversion of -dodecane also increases from 42% to 60% at 600°C and from 66% to 80% at 625°C. The coated zeolite can significantly inhibit the carbon deposition during supercritical cracking reactions.

关键词： HZSM-5     self-made ceramic-like     gas-aided     Conversion     Suspensoid    

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Erratum to: Self-sacrificial templating synthesis of flower-like nickel phyllosilicates and its application

《化学科学与工程前沿（英文）》 2022年 第16卷 第10期   页码 1531-1531 doi: 10.1007/s11705-022-2241-4

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Unconventional hydrodynamics of hybrid fluid made of liquid metals and aqueous solution under applied

Xu-Dong ZHANG, Yue SUN, Sen CHEN, Jing LIU

《能源前沿（英文）》 2018年 第12卷 第2期   页码 276-296 doi: 10.1007/s11708-018-0545-3

摘要： The hydrodynamic characteristics of hybrid fluid made of liquid metal/aqueous solution are elementary in the design and operation of conductive flow in a variety of newly emerging areas such as chip cooling, soft robot, and biomedical practices. In terms of physical and chemical properties, such as density, thermal conductivity and electrical conductivity, their huge differences between the two fluidic phases remain a big challenge for analyzing the hybrid flow behaviors. Besides, the liquid metal immersed in the solution can move and deform when administrated with non-contact electromagnetic force, or even induced by redox reaction, which is entirely different from the cases of conventional contact force. Owing to its remarkable capability in flow and deformation, liquid metal immersed in the solution is apt to deform on an extremely large scale, resulting in marked changes on its boundary and interface. However, the working mecha- nisms of the movement and deformation of liquid metal lack appropriate models to describe such scientific issues via a set of well-established unified equations. To promote investigations in this important area, the present paper is dedicated to summarizing this unconventional hydrodynamics from experiment, theory, and simulation. Typical experimental phenomena and basic working mechanisms are illustrated, followed by the movement and deformation theories to explain these phenomena. Several representative simulation methods are then proposed to tackle the governing functions of the electrohydrodynamics. Finally, prospects and challenges are raised, offering an insight into the new physics of the hybrid fluid under applied fields.

关键词： liquid metal     hybrid fluid     hydrodynamics     surface tension     applied fields     self-actuation    

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Solution properties and self-association of multi-blocks like copolymer P(AM/AA) prepared by template

ZHANG Yuxi, WU Feipeng, LI Miaozhen, WANG Erjian

《化学科学与工程前沿（英文）》 2007年 第1卷 第1期   页码 68-71 doi: 10.1007/s11705-007-0014-8

摘要： The association and properties of multi-block like copolymers (TP) of acrylamide (AM) and acrylic acid (AA) prepared by template copolymerization in aqueous solution were studied. The results showed that the copolymers of this type exhibited a significant structure effect compared with that of similar random copolymers (CP) obtained by copolymerization in the absence of template. Decreasing the value of pH or adding Ca ion to the copolymer solution will make phase separation occur. The TEM images demonstrated that the phase separation caused by Ca ion was due to the formation of extensively intermolecular cross-linking. With the increase of the pH value of copolymer solution, the changes of the solution viscosity was similar with that of homopolyacrylic acid, which originally increased and then decreased. But the increase range of template copolymer was higher than that of homopolyacrylic acid. TEM images indicated that at the maximal viscosity the copolymer obtained in the presence of template formed coiled aggregates.

关键词： aqueous solution     homopolyacrylic     copolymer solution     significant structure     presence    

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Self-sacrificial templating synthesis of flower-like nickel phyllosilicates and its application as high-performance

《化学科学与工程前沿（英文）》 2022年 第16卷 第4期   页码 484-497 doi: 10.1007/s11705-021-2074-6

摘要： The nanocomposites of flower-like nickel phyllosilicate particles incorporated into epoxy resin were fabricated via an in-situ mixing process. The flower-like nickel phyllosilicate particles were firstly synthesized using a mild self-sacrificial templating method, and the morphology and lamellar structure were examined carefully. Several properties of mechanical, thermal and tribological responses of epoxy nanocomposites were performed. It was demonstrated that adequate flower-like nickel phyllosilicate particles dispersed well in the matrix, and the nanocomposites displayed enhanced tensile strength and elastic modulus but decreased elongation at break as expected. In addition, friction coefficient and wear rate were increased first and then decreased along with the particle content, and showed the lowest values at a mass fraction of 5%. Nevertheless, the incorporated flower-like nickel phyllosilicate particles resulted in the continuously increasing thermal stability of epoxy resin (EP) nanocomposites. This study revealed the giant potential of flower-like particles in preparing high-quality EP nanocomposites.

关键词： nickel phyllosilicate     flow-like structure     mechanical property     thermal stability     tribological performance    

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Brazing of ceramic-to-ceramic and ceramic-to-metal joints in air

Kirsten BOBZIN, Thomas SCHLAEFER, Lidong ZHAO, Nils KOPP, Arne SCHLEGEL

《机械工程前沿（英文）》 2010年 第5卷 第2期   页码 125-129 doi: 10.1007/s11465-010-0007-z

摘要： Reactive air brazing (RAB) is an emerging technology for the production of ceramic-to-ceramic and ceramic-to-metal joints. In this study, RAB was investigated with respect to the potential applications for solid oxide fuel cells (SOFCs) as one example of use. It was found that alumina could be well brazed by RAB with AgCu and AgCuTi brazes. Both braze composition and brazing temperature influenced significantly the wetting behavior and their mechanism of wetting. AgCu and AgCuTi braze alloys could also be used to produce brazed joints with the SOFC materials ceramic yttria stabilized zirconia and steel X1CrTiLa22. However, CuO reacts with the steel, forming a brittle oxide layer on the steel surface, which is undesirable for SOFC applications. The first trials with Ag0.5Al showed a promising solution.

关键词： reactive air brazing (RAB)     X1CrTiLa22     Al2O3     yttria stabilized zirconia (YSZ)     solid oxide fuel cell (SOFC)    

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Chloride ingress and macro-cell corrosion of steel in concrete made with recycled brick aggregate

《结构与土木工程前沿（英文）》 2021年 第15卷 第6期   页码 1358-1371 doi: 10.1007/s11709-021-0769-x

摘要： An investigation on chloride ingress and macro-cell corrosion of steel bars in concrete made with recycled brick aggregate (RBA) was carried out. As control cases, virgin brick aggregate (BA) and stone aggregate (SA) were also investigated. Both cylindrical and cracked prism specimens were studied for 16 different cases. The prism specimens were made with a segmented steel bar providing electrical connection from outside of the specimens to measure macro-cell corrosion current continuously under seawater splash exposure for a period of 30 d using a data logger. Cylindrical specimens were submerged in 3% NaCl solution at a temperature of 40°C to investigate chloride ingress in concrete made with RBA, BA, and SA after 120 and 180 d. Half-cell potential, corrosion area, and depths of corrosion were also investigated. The chloride ingress as well as corrosion of steel bars in concrete made with the different types of aggregate is ordered as RBA > BA > SA.

关键词： brick aggregate     chloride ingress     macro-cell corrosion     recycled brick aggregate    

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Ceramic membrane fouling mechanisms and control for water treatment

《环境科学与工程前沿（英文）》 2023年 第17卷 第10期 doi: 10.1007/s11783-023-1726-9

摘要：

● The fouling is summarized based on ceramic membrane performance and pollutants.

关键词： Ceramic membrane     Fouling model     Fouling control    

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以旋涡塔阵建立速成及高效益的人工防护林带 化整片沙漠为大片绿地

严隽森

《中国工程科学》 2003年 第5卷 第5期   页码 24-30

摘要：

改造沙漠、利用沙漠，必须在沙漠中建立多道防护林带，才可大力推展沙产业、改良沙漠环境、并逐步化整片沙漠为大片绿地。对此，目前世界各国均束手无策或认为不可能。文章建议以旋涡塔阵及流体力学中的旋涡破裂特性及与镇定仓等的相互干扰，将塔阵后方的强风变为湍流弱风，而建立速成及高效益的人工防护林带；适当的重量分布在各镇定仓内，可使旋涡塔阵在狂风中仍屹立不移，在弱风区中，可大力推展沙产业，并与多方面的专家合力，适度开发利用沙漠；化整片沙漠为大片绿地，化荒芜及有严重危害的沙漠为宝地，并可在沙漠中以旋涡塔阵，保护长期及深层探勘的工作区，以利于发现及测定深埋地下的世界级的矿藏。

关键词： 旋涡塔阵     人工防护林带     沙产业    

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Experimental and computational assessment of 1,4-Dioxane degradation in a photo-Fenton reactive ceramic

《环境科学与工程前沿（英文）》 2021年 第15卷 第5期 doi: 10.1007/s11783-020-1341-y

摘要：

• 1,4-Dioxane was degraded via the photo-Fenton reactive membrane filtration.

关键词： Photo-Fenton     Ceramic membrane     1     4-Dioxane     Goethite    

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Advances in polishing of internal structures on parts made by laser-based powder bed fusion

《机械工程前沿（英文）》 2023年 第18卷 第1期 doi: 10.1007/s11465-022-0724-0

摘要： The internal structures of metallic products are important in realizing functional applications. Considering the manufacturing of inner structures, laser-based powder bed fusion (L-PBF) is an attractive approach because its layering principle enables the fabrication of parts with customized interior structures. However, the inferior surface quality of L-PBF components hinders its productization progress seriously. In this article, process, basic forms, and applications relevant to L-PBF internal structures are reviewed comprehensively. The causes of poor surface quality and differences in the microstructure and property of the surface features of L-PBF inner structures are presented to provide a perspective of their surface characteristics. Various polishing technologies for L-PBF components with inner structures are presented, whereas their strengths and weaknesses are summarized along with a discussion on the challenges and prospects for improving the interior surface quality of L-PBF parts.

关键词： laser-based powder bed fusion     polishing     internal structures     surface quality     surface features     post process     additive manufacturing    

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Compressive behavior and energy absorption of polymeric lattice structures made by additive manufacturing

Sheng WANG, Jun WANG, Yingjie XU, Weihong ZHANG, Jihong ZHU

《机械工程前沿（英文）》 2020年 第15卷 第2期   页码 319-327 doi: 10.1007/s11465-019-0549-7

摘要： Lattice structures have numerous outstanding characteristics, such as light weight, high strength, excellent shock resistance, and highly efficient heat dissipation. In this work, by combining experimental and numerical methods, we investigate the compressive behavior and energy absorption of lattices made through the stereolithography apparatus process. Four types of lattice structures are considered: (i) Uniform body-centered-cubic (U-BCC); (ii) graded body-centered-cubic (G-BCC); (iii) uniform body-centered-cubic with -axis reinforcement (U-BCCz); and (iv) graded body-centered-cubic with -axis reinforcement (G-BCCz). We conduct compressive tests on these four lattices and numerically simulate the compression process through the finite element method. Analysis results show that BCCz has higher modulus and strength than BCC. In addition, uniform lattices show better energy absorption capabilities at small compression distances, while graded lattices absorb more energy at large compression distances. The good correlation between the simulation results and the experimental phenomena demonstrates the validity and accuracy of the present investigation method.

关键词： lattice structure     polymer     compressive behavior     additive manufacturing     simulation    

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Dynamical research on spherical micro actuator with piezoelectric ceramic stacks drivers

ZHANG Ruihua, CHEN Haichu

《机械工程前沿（英文）》 2007年 第2卷 第4期   页码 433-438 doi: 10.1007/s11465-007-0074-y

摘要： This paper develops a 30 mm × 30 mm × 50 mm spherical micro actuator driven by piezoelectric ceramic stacks (PZT), and analyzes its dynamic performances. First, the space coordinate relationship of the spherical micro actuator and a dynamic model are set up. Second, The Runge-Kutta arithmetic is used to calculate the dynamical parameters of the micro actuator; the SIMULINK module of MATLAB is used to build the dynamical simulating model and then simulate it. Third, an experimental sample of the spherical micro actuator is developed, a micromanipulator is integrated with a micro-gripper based on the sample spherical micro actuator, and the experimental research on the micro assembly is conducted between a micro shaft of 180 μm and a micro spindle sleeve of 200 μm. Finally, the characteristics of the spherical micro actuator influenced by the mass of the metal sphere of the micro actuator, driving signal frequency, friction coefficient of the contact surface between the metal sphere and the friction block of the micro driving unit are analyzed. The experimental results indicate that the rotation resolution of the micro actuator reaches 0.000 1°, the rotation positioning precision reaches 0.000 5°, and the maximum working frequency is about 1200 Hz. The experimental results validate the back rotation vibration model of the spherical micro actuator. The micromanipulator integrated by the spherical micro actuator can meet the requirements of precise micro operation and assembly for micro electro mechanical systems (MEMS) or other microelements in micro degree fields.

关键词： spherical     micro-gripper     friction coefficient     dynamic     frequency    

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面向绿色化工应用的陶瓷催化膜反应器的设计与制备 Feature Article

张广儒, 金万勤, 徐南平

《工程（英文）》 2018年 第4卷 第6期   页码 848-860 doi: 10.1016/j.eng.2017.05.001

摘要：

催化膜反应器将反应和分离耦合在一个单元，在化工生产中被视为一种绿色的化工新工艺。而在催化膜反应器中采用陶瓷膜可以使膜反应器的应用范围扩展到一些苛刻环境。本文介绍了基于气体分离的致密陶瓷催化膜反应器和基于非均相体系分离的多孔陶瓷催化膜反应器，评述了近10 年两种不同种类的膜反应器的最新进展以及本课题组的相关工作。面向能源、环境领域的应用，对膜反应器的设计、制备及应用展开重点讨论。针对各个膜反应器，从膜及膜反应器构型入手，以典型的催化反应为例，对膜反应器的设计及优化进行详细论述，最后探讨了进一步发展所面临的瓶颈和可能取得突破的方向，以及膜与膜反应器未来发展应重点关注的领域。

关键词： 致密膜     多孔膜     催化膜反应器     气体分离     非均相催化    

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Enhanced cross-flow filtration with flat-sheet ceramic membranes by titanium-based coagulation for membrane

《环境科学与工程前沿（英文）》 2022年 第16卷 第8期 doi: 10.1007/s11783-022-1531-x

摘要：

• Ceramic membrane filtration showed high performance for surface water treatment.

关键词： Ceramic membrane     Coagulation     Polytitanium chloride     Membrane fouling    

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标题 作者 时间 类型 操作

Catalytic cracking of endothermic fuels in coated tube reactor

LI Jia, ZOU Jijun, ZHANG Xiangwen, GUO Wei, MI Zhentao

期刊论文

Erratum to: Self-sacrificial templating synthesis of flower-like nickel phyllosilicates and its application

期刊论文

Unconventional hydrodynamics of hybrid fluid made of liquid metals and aqueous solution under applied

Xu-Dong ZHANG, Yue SUN, Sen CHEN, Jing LIU

期刊论文

Solution properties and self-association of multi-blocks like copolymer P(AM/AA) prepared by template

ZHANG Yuxi, WU Feipeng, LI Miaozhen, WANG Erjian

期刊论文

Self-sacrificial templating synthesis of flower-like nickel phyllosilicates and its application as high-performance

期刊论文

Brazing of ceramic-to-ceramic and ceramic-to-metal joints in air

Kirsten BOBZIN, Thomas SCHLAEFER, Lidong ZHAO, Nils KOPP, Arne SCHLEGEL

期刊论文

Chloride ingress and macro-cell corrosion of steel in concrete made with recycled brick aggregate

期刊论文

Ceramic membrane fouling mechanisms and control for water treatment

期刊论文

以旋涡塔阵建立速成及高效益的人工防护林带 化整片沙漠为大片绿地

严隽森

期刊论文

Experimental and computational assessment of 1,4-Dioxane degradation in a photo-Fenton reactive ceramic

期刊论文

Advances in polishing of internal structures on parts made by laser-based powder bed fusion

期刊论文

Compressive behavior and energy absorption of polymeric lattice structures made by additive manufacturing

Sheng WANG, Jun WANG, Yingjie XU, Weihong ZHANG, Jihong ZHU

期刊论文

Dynamical research on spherical micro actuator with piezoelectric ceramic stacks drivers

ZHANG Ruihua, CHEN Haichu

期刊论文

面向绿色化工应用的陶瓷催化膜反应器的设计与制备

张广儒, 金万勤, 徐南平

期刊论文

Enhanced cross-flow filtration with flat-sheet ceramic membranes by titanium-based coagulation for membrane

期刊论文